MS Report from Instrument: LCMS-02 File ..0613 2017-06-13 08-41-18\\BIZ2017-613-WYQ9.D Tgt Mass (CHM): Injection Date : 13 Jun 17 12:05 pm +0800 Seq. Line : 43 Sample Name : BIZ2017-613-WYQ9 Location : P1-B-03 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170613\\20170613 2017-06-13 08-41-18\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170613\\20170613 2017-06-13 08-41-18\\1-POS-3MIN.M Catalog No : HY-14199 Batch#24919 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off 50040030020010000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7080000060000040000020000000.511.5 Ion 224.1, MSD1 224.1,Target Mass 223.1 +H Positive, EIC=223.8:224.8 3002502001501005000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min22.5min1.2121.4621.184mAU1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.18 0.02 723.32 610.10 99.71 188 1.46 0.03 2.11 1.14 0.29 188 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.05 2479061.75 821467.75 100.00 188LCMS-02 6/13/2017 14:23:06 CLJ_701Page 1 of 2
MS Report from Instrument: LCMS-02Ret. Time: 1.21 <<<< POSITIVE SPECTRA >>>> ES-API Positive 188.2 1.2250000200000150000100000500000200300400500600700800900m/zLCMS-02 6/13/2017 14:23:06 CLJ_701Page 2 of 2
